Pittchem NMR http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news PITTCHEM NMR Instrument Status Tue, 10 Jan 2012 12:00:00 -0500 http://blogs.law.harvard.edu/tech/rss New Autosampler Installations PITTCHEMNMR081 Tue, 10 Jan 2012 12:00:00 -0500 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news
Starting Tuesday, January 10th, at noon, autosamplers will be installed on both 300MHz NMR instruments. Both autosamplers will be controlled by the IconNMR automation software. Instructions for using both instruments are available on the NMR website: http://www.chem.pitt.edu/facilities/nmr- spectroscopy-0 .

The time limits on the instruments will be as follows:

301B (13th Floor)
Daytime Hours: 8 AM - 11 PM
Daytime limit: 15 minutes
Nighttime Hours: 11PM - 8 AM
Nighttime limit: 4 hours

Nighttime experiments can be submitted in advance to the system. Instructions for submitting nighttime experiments on the 301b are available online in the guide "Using the SampleExpress".

300 (4th Floor)
Daytime Hours: 8 AM - 10 PM
Daytime limit: 15 minutes
Nighttime Hours: 10 PM - 8 AM
Nighttime limit: 11 hours

Due to hardware limitations, night experiments cannot be submitted before 10 PM to NMR 300. Thus, we will continue to use the FACES scheduling system to schedule night time on this instrument. Instructions for how to set up nighttime experiments on this NMR 300 are posted online in the guide "Using the NMRCase".


Additionally, some aspects of the 400A policy will be changed:

Nighttime experiments can be submitted in advance to the system.. Instructions for submitting nighttime experiments on the 301b are available online in the guide "Using the SampleExpress".

400A:
The nighttime hours will remain the same as before, 9PM - 9AM.
The daytime time limit will increase to 30 minutes per sample.
Please contact the NMR Facility if there are any questions or concerns about the operation or policies of the new autosamplers.
]]> 400A Autosampler Repaired PITTCHEMNMR080 Fri, 18 Nov 2011 14:42:05 -0500 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news 13C Available on 4th Floor NMR PITTCHEMNMR079 Wed, 07 Sep 2011 16:01:05 -0400 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news 13C unavailable on 4th Floor NMR PITTCHEMNMR078 Thu, 01 Sep 2011 16:11:05 -0400 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news Autosampler Repaired on 400A PITTCHEMNMR077 Thu, 21 Jul 2011 11:05:05 -0400 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news Autosampler Out of Order, 400A is Walk-On PITTCHEMNMR075 Thu, 16 Jun 2011 10:14:05 -0400 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news 500 Probe Repairs Complete PITTCHEMNMR074 Thu, 05 May 2011 15:57:05 -0400 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news 4th Floor NMR Available PITTCHEMNMR073 Wed, 27 Apr 2011 15:04:05 -0500 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news 700 Autosampler PITTCHEMNMR072 Thu, 03 Mar 2011 17:06:05 -0500 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news Time Limits on 400A Autosampler PITTCHEMNMR071 Tues, 22 Feb 2011 16:19:05 -0500 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news During the daytime hours, the previous limit of 3 hours per research group per day has been lifted. Individual users are still limited to 15 min/experiment but there are no longer any daily group limits.]]> 4th Floor 300 Unavailable February 23 PITTCHEMNMR070 Tue, 22 Feb 2011 16:19:05 -0500 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news 600 Probe Upgrade PITTCHEMNMR069 Tue, 27 Feb 2011 16:19:05 -0500 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news Some experiments unavailable on 500MHz PITTCHEMNMR068 Tue, 22 Jan 2011 9:15:05 -0500 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news Automatic tuning and matching using the "atma" command is also unavailable. Tuning and matching can only be performed manually.]]> Autosampler available PITTCHEMNMR067 Thu, 14 Nov 2010 14:18:05 -0500 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news NMR Facility Upgrade Complete PITTCHEMNMR066 Wed, 08 Dec 2010 11:15:05 -0500 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news Autosampler unavailable, NMR 400A is walk-on PITTCHEMNMR065 Tue, 30 Nov 2010 13:43:05 -0500 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news NMR 400A available PITTCHEMNMR064 Mon, 29 Nov 2010 17:12:05 -0500 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news NMR 400A not available PITTCHEMNMR063 Mon, 29 Nov 2010 16:22:05 -0500 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news Change in scheduling policy for 4th floor NMR PITTCHEMNMR062 Fri, 19 Nov 2010 14:36:05 -0500 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news New 31P experiments available on 400B PITTCHEMNMR061 Fri, 19 Nov 2010 14:36:05 -0500 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news Upcoming installation of autosampler on 400A this Thursday PITTCHEMNMR060 Tue, 09 Nov 2010 2:27:05 -0500 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news http://www.chem.pitt.edu/facilities/nmr-spectroscopy-0 .

Scheduling for the 400A will be handled by the ICON-NMR software. The online FACES schedule will no longer be used for this instrument. The time limits will initally be set as follows:

Daytime (8AM - 8PM):
Maximum 15 min per experiment
Limit of 3 hours per research group/per day

Night (8PM - 8AM)
Limit of 6 hours per research group/per day
]]> 301B Unavailable this weekend PITTCHEMNMR059 Fri, 29 Oct 2010 13:17:05 -0400 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news New computer for NMR 301B PITTCHEMNMR058 Tue, 12 Oct 2010 11:21:05 -0400 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news 500 available PITTCHEMNMR057 Tue, 28 Sep 2010 10:57:05 -0400 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news All current users of the 300MHz and 400MHz instruments will be automatically given access to the 500MHz; no extra training is required.
The procedure for using the 500MHz is very similar to the procedure for the 400MHz instruments; a guide outlining the 500MHz procedure will be posted by the instrument.
Time on the 500 will be available in fifteen minute increments, up to a maximum appointment length of 1hr during the day. Overnight time will run from 10PM to 8AM. ]]> 4th Floor NMR reservations for fall semester PITTCHEMNMR056 Wed, 22 Sep 2010 12:31:05 -0400 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news Thursday 9/23, 2:30pm
Tuesday 9/28, 2:30pm and 7pm
Thursday 9/30, 2:30pm
Tuesday 10/5, 2:30pm and 7pm
Thursday 10/7, 2:30pm
Tuesday 10/26, 2:30pm and 7pm
Thursday 10/28, 2:30pm
Each of these lab sessions will last about 1.5 hours, please plan accordingly. ]]> 400A available PITTCHEMNMR055 Mon, 16 Aug 2010 11:47:05 -0400 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news 301A de-energized, 4th Floor 300 walk-on PITTCHEMNMR054 Mon, 12 Jul 2010 12:30:05 -0400 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news NMR 300 on the 4th floor is available for walk-on use. ]]> 301A to be de-energized PITTCHEMNMR053 Fri, 09 Jul 2010 10:48:05 -0400 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news 119Sn NMR available on 400B PITTCHEMNMR052 Tue, 06 Jul 2010 13:12:05 -0400 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news 400B Available PITTCHEMNMR051 Tue, 15 Jun 2010 15:50:02 -0400 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news 400B Unavailable PITTCHEMNMR050 Mon, 14 Jun 2010 10:54:06 -0400 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news 7Li experiments available on 400B PITTCHEMNMR049 Thu, 20 May 2010 16:52:02 -0400 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news 11B experiments available on 400B PITTCHEMNMR048 Tue, 18 May 2010 16:23:02 -0400 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news Both 400MHz instruments available PITTCHEMNMR047 Fri, 14 May 2010 13:25:21 -0400 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news
During the day, the maximum appointment time is 1 hour. Overnight time runs from 10PM to 8AM. Instructions for using the new instruments are posted near the computers.

The 400A is equipped with a 13C/1H dual channel observe probe which provides excellent carbon sensitivity. The 400A has parameter sets for the 1H, 13C, DEPT135, COSY, NOESY, HMQC, and HMBC experiments.

The 400B is equipped with a broadband observe probe, which can be tuned to nuclei other than 13C, including 19F. The 400B has parameter sets for the 1H, 13C, 19F, 31P, DEPT135, COSY, NOESY, HMQC, and HMBC experiments.]]> 600 Available PITTCHEMNMR046 Tue, 11 May 2010 13:35:21 -0500 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news New 400 MHz NMR available PITTCHEMNMR045 Fri, 30 Apr 2010 10:45:21 -0500 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news
Instructions for using the new instrument will be posted near the 400A computer.

The 400A has parameter sets for the 1H, 13C, DEPT135, COSY, NOESY, HMQC, and HMBC experiments.]]> 301 to be de-energized PITTCHEMNMR044 Tue, 27 Apr 2010 10:44:21 -0500 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news 600 Unavailable PITTCHEMNMR043 Wed, 21 Apr 2010 15:58:52 -0500 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news All Experiments Available on 600 PITTCHEMNMR042 Tue, 30 Mar 2010 10:21:52 -0500 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news 301A Available PITTCHEMNMR041 Mon, 29 Mar 2010 12:32:12 -0500 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news 600 MHz Issue PITTCHEMNMR040 Mon, 22 Mar 2010 17:15:22 -0400 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news NMR Sample Tube Reminder PITTCHEMNMR039 Fri, 19 Mar 2010 16:51:22 -0500 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news 301A Unavailable PITTCHEMNMR038 Fri, 19 Mar 2010 16:51:22 -0500 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news 301B available for short-term experiments PITTCHEMNMR037 Mon, 15 Mar 2010 14:40:56 -0500 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news Upcoming Changes to 300MHz Instruments PITTCHEMNMR036 Wed, 03 Mar 2010 10:37:41 -0500 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news 600 Available PITTCHEMNMR035 Tue, 02 Mar 2010 14:24:59 -0500 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news 600 Unavailable - Compressor Issue PITTCHEMNMR034 Mon, 01 Mar 2010 11:04:10 -0500 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news 500 MHz Decommissioned Wed, 10 Feb 2010 17:25:32 -0500 PITTCHEMNMR033 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news NMR Data Server Problems PITTCHEMNMR032 Thu, 21 Jan 2010 14:08:04 -0500 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news Topshim available for NMR 301 PITTCHEMNMR031 Thu, 21 Jan 2010 14:08:04 -0500 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news Topshim not available on 301 PITTCHEMNMR030 Wed, 13 Jan 2010 16:56:58 -0500 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news NMR Server Access from NMR Lab Computers PITTCHEMNMR029 Fri, 18 Dec 2009 10:38:25 -0500 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news 700 fully available; 5mm probe in use PITTCHEMNMR028 Tue, 13 Oct 2009 14:46:47 -0400 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news 700 Available for short-term experiments PITTCHEMNMR027 Wed, 16 Sep 2009 14:20:24 -0400 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news 700 Unavailable PITTCHEMNMR026 Wed, 19 Aug 2009 12:50:32 -0400 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news 500 Scheduling Changes PITTCHEMNMR025 Fri, 31 Jul 2009 16:11:00 -0400 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news 301A and 300 Shimming PITTCHEMNMR024 Tue, 21 Jul 2009 11:34:47 -0400 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news 500 Spinning Fixed PITTCHEMNMR023 Wed, 15 Jul 2009 09:48:40 -0400 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news 301A Fixed PITTCHEMNMR022 Wed, 01 Jul 2009 09:48:17 -0400 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news 301A unavailable PITTCHEMNMR021 Thu, 25 Jun 2009 16:51:59 -0400 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news Out of office PITTCHEMNMR020 Mon, 22 Jun 2009 11:19:05 -0400 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news 700 Available PITTCHEMNMR019 Tue, 02 Jun 2009 10:53:05 -0400 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news 700 Unavailable PITTCHEMNMR018 Mon, 01 Jun 2009 11:12:36 -0400 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news 700 Unavailable PITTCHEMNMR017 Fri, 01 May 2009 08:59:42 -0400 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news Long-term Carbon NMR PITTCHEMNMR016 Fri, 24 Apr 2009 09:48:01 -0400 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news Accessing 4th Floor NMR PITTCHEMNMR015 Wed, 22 Apr 2009 15:20:22 -0400 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news 500 Available PITTCHEMNMR014 Fri, 10 Apr 2009 15:56:31 -0400 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news 19F and 31P Expts on 301 Available PITTCHEMNMR013 Mon, 06 Apr 2009 10:16:13 -0400 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news 500 Unavailable PITTCHEMNMR012 Fri, 06 Mar 2009 09:02:11 -0500 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news 300 Available PITTCHEMNMR011 Wed, 25 Mar 2009 13:04:13 -0500 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news 300 Unavailable PITTCHEMNMR010 Fri, 20 Mar 2009 09:48:02 -0500 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news 19F and 31P Experiments on 301 PITTCHEMNMR009 Tue, 17 Mar 2009 13:38:24 -0500 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news 700 Available PITTCHEMNMR008 Mon, 16 Mar 2009 13:47:16 -0500 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news 700 Unavailable PITTCHEMNMR007 Wed, 11 Mar 2009 09:25:45 -0500 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news 301B Available PITTCHEMNMR006 Tue, 03 Mar 2009 16:21:35 -0500 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news 301B Unavailable PITTCHEMNMR005 Mon, 02 Mar 2009 11:24:37 -0500 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news 301B Available PITTCHEMNMR004 Fri, 27 Feb 2009 11:23:20 -0500 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news 301B Unavailable PITTCHEMNMR003 Thu, 26 Feb 2009 18:19:46 -0500 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news 11B and 29Si on 301B PITTCHEMNMR002 http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news Thu, 26 Feb 2009 14:14:48 -0500 700 Unavailable http://www.chem.pitt.edu/facilities/nmr-spectroscopy/news PITTCHEMNMR001 Thu, 19 Feb 2009 10:34:01 -0500